The influence of variations in desorption temperature, desorption fl ow and sample preparation on VDA 278 analysis method [1] robustness and reproducibility is studied using a wide variety of samples from automobile interior materials: polypropylene (PP) granulate, polyurethane (PU) foam, leather, Duroplastic plastics and paint. It is shown that a temperature difference of just two degrees at 90°C or at 120°C can lead to an emission deviation of ± 20 percent. Also, desorption flow is shown to have significant influence on paint stripe emission values while there is little influence on samples like PP granulate.

A software feature “VDA 278 calibration” is presented, which enables temperature calibration by just a few mouse-clicks. Examples shown are adjustment of the temperature to 90°C and 120°C respectively as required in the VDA 278 method, with a deviation smaller than ± 1.0°C.

Thermal Desorption System (TDS)

The GERSTEL Thermal Desorption System (TDS) is a flexible multi-functional system for highly sensitive determination of volatile and semi-volatile organic compounds (VOCs and SVOCs) that have been trapped on adsorbent tubes or on GERSTEL Twisters.

The TDS is also frequently used for direct thermal extraction and determination of VOCs and SVOCs from solids without sample preparation. Application examples are natural products, flavor and fragance, emssions from materials that are used indoors in buildings or in automobiles, semiconductors, polymers and packaging.